Nitric Acid, ASTM A, Practice C, (Huey Test) The specimens are boiled for five periods, each of 48 hours, in a 65 per cent solution of nitric acid. The corrosion. employed to measure the relative susceptibility of austenitic stainless steels to intergranular attack. ASTM A Practice C, boiling nitric acid test is also known . Ferric Sulfate – Sulfuric Acid, ASTM A – Practice B (Stretcher Test). Ferric Sulfate Nitric Acid, ASTM A, Practice C, (Huey Test). Nitric Acid, ASTM A

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Duplicate samples from both sides of a sheet sample are evaluated to determine if carburization results in intergranular attack. A recent publication on intergranular corrosion. Classification of the structure after A Practice A analysis will determine if the material is acceptable or if additional testing is required.

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The test is generally performed for acceptance of materials, but not sufficient for rejection of materials. Like what you saw? A different ASTM A test method must be used to quantify the level of corrosion or to disqualify a material for use. Please share this page: If materials with incorrect heat treatment enter service, they are liable to crack or fail by intergranular corrosion IGC much more rapidly than properly treated materials; ASTM A is a screening test to help find batches that are incorrectly processed.

See Appendix X1 for information regarding test selection.

In SEM analysis, intergranular corrosion is clear by the dark lines where the grain boundaries are eaten away. For example, in highly oxidizing solutions, intergranular attack can occur due to intermetallic phases, while attack of carbides may occur somewhat less oxidizing solutions. The Oxalic Acid test is only used to ensure that no corrosion exists; samples are labeled either “Acceptable” or “Suspect”. The inch-pound equivalents are in parentheses and may be approximate.

Historical Version s – view previous versions of standard Work Item s – proposed revisions of this standard Translated Version s: Metals like stainless steels and aluminum contain elements such as niobium and chromium, often integrated because of their natural corrosion resistance.

In many cases we can reduce that to as little as 24 hours more than the required testing time if you need fast results. The Copper Sulfate Test is especially effective for determining susceptibility to intergranular attack for low carbon steels. From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using state-of-the-art equipment. Share on Tumblr Print. Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice.


ASTM A Intergranular Corrosion Testing and Analysis

This method is a hour boiling test for “as received” specimens of stainless steel. How do you select the right ASTM corrosion testing method for your material? Intergranular corrosion shows up as the dark black lines around the grain boundaries.

Please specify the maximum allowable corrosion rate and any available data on the sensitizing heat treatment performed. Work Item s – proposed revisions of this standard. Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion. Each ASTM A Practice specification includes a list of the grades of stainless steels and the acceptable etch structures for the specific alloys.

This practice includes boiling the sample pracice 24 to hours in the solution above, and measures the materials performance quantitatively. Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.

It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. sstm

Corrosion Testing

In everyday applications, corrosion varies by materials and solutions. G2MT Labs is one of the few labs to offer all five ASTM A corrosion testing x262, as well as the expertise to help you parctice which tests to use, what atm do if a test fails, and other corrosion consulting as needed. ASTM does not give any warranty express or implied or make any representation that the contents of this abstract are accurate, complete or up to date. Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard.

Some specific hazards statements are given in Please refer to the specification for more details. This simple etching technique is used as a quick screening praactice to ensure that a material is free of intergranular corrosion susceptibility. Practice F, is a hour weight-loss based analysis that provides a quantitative measure of the materials performance, and is commonly used to analyze as-received stainless steels.


View more articles about Aerospace Oil and Gas Transportation. It depends on which Practice is selected, but typically ranges from to days for different tests.

Practice A, the oxalic acid etch test is used as a rapid technique to screen samples of certain stainless steel grades to ensure they are not susceptible to intergranular attack sensitization.

Choosing the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself.

The ASTM A tests can determine if the proper heat treatment was performed or if the alloys are in danger of intergranular corrosion occurring in use. Based on your materials, application, and requirements, the other 4 methods provide specific focuses. This method is preferable for chromium depletions and corrosion in intermetallic phases.

Intergranular Corrosion Testing: An Overview of ASTM A262

This test is used exclusively to determine corrosion in areas high in chromium carbide formations, and is not as effective for intergranular attack caused by other means. The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of elements such as Nb and Ti, or the effectiveness of reducing carbon content to resist intergranular attack.

All five methods within this specification involve exposing specimens to a chemical mixture designed to encourage corrosive behavior.

For example, many low-carbon and stabilized stainless steels e. ASTM A testing is a popular method of choice due to the variety of practices available and the relatively short turnaround for ppractice. Discover perspectives, resources, and advice from our world-leading Engaged Experts. If you are not sure, please contact us for assistance.

This abstract is a brief summary of the referenced standard. These tests are often run as a qualification test to ensure each batch of stainless steel is properly prepared. The bent samples are examined at low magnification, where the appearance of practicd or fissures indicate intergranular attack. This specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels.